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Certificate of Analysis · Standard specification

Phenol-d1 COA

Certificate of Analysis and technical specification for Phenol-d1 — CAS 1003-66-3. Applies to all consignments of this product and grade.

Product NamePhenol-d1
C.A.S. Number1003-66-3
Product CategoryLaboratory & Analytical Reagents
Product GroupDeuterated NMR Solvents
Grade / Standard95%(Isotopic)
Physical FormClear colorless liquid
Country of OriginIndia
PackingStandard export packing — bags, drums, carboys, IBC or ISO tank as applicable
StorageCool, dry, well-ventilated place in tightly closed original packing

Analytical Specification

S. No.Test ParameterSpecificationTypical ResultMethod
1DescriptionClear colorless liquidCompliesVisual
2IdentificationConforms to the structure of the substanceCompliesFTIR / Chemical test
3AssayNot less than 95.0 % w/w95.44Titrimetry / Instrumental
4Purity (by GC)Not less than 99.5 % (area)99.89Gas Chromatography
5Colour (APHA / Pt-Co)Not more than 106ASTM D1209
6Water ContentNot more than 0.05 % w/w0.0114Karl Fischer titration
7Acidity (as acetic acid)Not more than 0.002 % w/w0.0004Titrimetry
8Residue on EvaporationNot more than 0.001 % w/w0.0002Gravimetry
9Specific Gravity at 25 °CAs per specificationConformsPycnometry / ASTM D4052
10Refractive Index at 20 °CAs per specificationConformsRefractometry / ASTM D1218

This document sets out the standard specification for Phenol-d1 and applies to all consignments of this grade. It is not a lot-specific release document; a lot-specific certificate carrying the analysis of the material actually shipped is issued with each consignment. Scapex Exports supplies against customer-specified assay limits and pharmacopoeial standards — send your specification sheet and we will confirm compliance before order.

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